Friday 17 August 2012

HOW TO WRITE YOUR HS CHEMISTRY PROJECT

                                                
CHEMISTRY   PROJECT  WORK
ON
DETECTION   OF    ADULTERANTS    IN   SOME   COMMON FOOD STUFFS

                             SUBMITTED TO
THE DEPARTMENT OF CHEMISTRY
DARRANG COLLEGE, TEZPUR






BY

DHRUBA JYOTI NATH
ROLL NO.-10B0297, Sec-A
H.S 2nd YEAR (SCIENCE)
PREFACE

                 This is my H.S 2nd year chemistry project .I have put my sincere efforts in it. The main objective of the project is to detect some common food adulterants present in different food stuffs. I have tried my best in explaining the aspects of different food adulterants and their effects. In spite of my efforts, there may be some omission or mistakes and suggestions to improve it will be duly noted. Thank you.




                                                            

    Date:                  SIGNATURE:
                                                  (DHRUBA JYOTI NATH)



            ACKNOWLEDGEMENT

                    I would like to take this opportunity to express my sincere gratitude to my Chemistry teacher DR. PALASMONI SAIKIA for his vital support ,guidance & encouragement ­­- without which this project would not have come forth .My sincere gratitude also goes to my  mother for providing me with the food stuffs. I would also like to express my gratitude to the chemistry bearers who provided me with the laboratory equipments and the required chemicals during the making of this project.                                                                                                                              









               

CONTENTS
CHAPTER
                       UNITS
PAGE NO.
1
1.1 INTRODUCTION                        FIG.1                                                  1.2 THEORY
2                                         3                          3
2
2.1 DETECTION OF ARGEMONE OIL IN MUSTARD OIL -                                          FIG. 1                                                                             2.2 DETECTION OF VANASPATI IN DESI GHEE-                                       FIG. 2                                                        2.3 DETECTION OF STARCH INMILK                                                 2.4 DETECTION OF METANIL  YELLOW IN TURMERIC POWDER            2.5 DETECTION OF ADULTERANTS IN CHILLY POWDER                           2.6 DETECTION OF DUST PARTICLES IN ATTA          
6
6
7
8
9
11

13
15
3
ADDITIONAL ADULTERANTS
17
4
CONCLUSION
19
5
REFERENCE
21


























1.1            INTRODUCTION
                 Adulteration in food is normally present in its most crude form; prohibited substances are either added partly or wholly substituted. Normally the contamination/adulteration in food is done either for financial gain or due to carelessness and lack in proper hygienic and condition of processing, storing, transportation and marketing. This ultimately results that the consumer is either cheated or often become victim of diseases. Such type of adulteration is quite common in developing countries or backward countries.                                             
                             It is associated with the profit of making business. So, they are substances of cheap quality and dangerous to our health .Adulteration is the act of intentionally debasing the quality of food offered for sale either by mixture or substitution of inferior substances or by the removal of some valuable ingredient. In the past few decades adulteration of food has become one of the most serious problems.                             Fig-1.1
                      Consumption of adulterated food causes diseases like cancer, asthma, ulcer, etc. Majority of adulterants used by the shopkeepers are cheap substitutes which are easily available.
                In order to prevent adulteration of food products by dishonest traders, the government has issued ‘The Prevention of Food Adulteration Act’. The Bureau of   Indian Standards is the agency in India that provides the certificate of reliability to food manufacturers in India.
.
1.2                THEORY 
                The increasing number of food producers and the outstanding amount of import foodstuffs enable the producers to mislead and cheat consumers. To food                                                                                                                                                                                                                                                                                        
adulteration is very difficult. The consciousness of consumers would be crucial. Ignorance and unfair market behavior may endanger consumer health and misleading can lead to poisoning.                                                                                
                    In the past few decades, adulteration of food has become one of the serious problems. Consumption of adulterated food causes serious diseases like cancer, diarrhea, asthma, ulcers, etc. Majority of fats, oils and butter are paraffin wax, castor oil and hydrocarbons. Red chili powder is mixed with brick powder and pepper is mixed with dried papaya seeds. These adulterants can be easily identified by simple chemical tests.            
                    Several agencies have been set up by the Government of India to remove adulterants from food stuffs.   
                    AGMARK - acronym for agricultural marketing....this organization certifies food products for their quality. Its objective is to promote the Grading and Standardization of agricultural and allied commodities.
                                                                                                                                                                                                     

  2.1DETECTION OF      ARGEMONE OIL IN MUSTARD OIL      
        Argemone is a non-edible oil which is used to adulterate vegetable oil or fat. It is extracted from the prickly poppy flower. It is cheaper than mustard oil and gives economic profit. But it is harmful and is responsible for the dropsy   disease in human beings in which the different parts of the body swells out. So the detection of argemone oil is carried out in the following manner……..

. FIG2                           
EXPERIMENT NO. 1
REQUIREMENTS:  (i) A test tube (ii) Conc. HNO3 (iii) Sample
PROCEDURE:. Take a small amount of oil in a test tube. Add a few drops of conc. HNO3 and shake. Appearance of red color indicates the presence of argemone oil.
ASSAM VALLEY MUSTARD OIL, BATCH NO. 1901/7810/B3,MANUFACTURED DATE:AUG/11
DHARA,BATCH NO.1701/6102/B2,MANUFACTURED DATE:NOV/11
ADULTERANTS FOUND
ADULTERANTS NOT FOUND
                                                                                                                                                                                                                                                                                              
    2.2 DETECTION OF VANASPATI IN DESI GHEE
            Desi ghee, which is a milk product, is much costlier than vanaspati ghee. So desi ghee is often adulterated with vanaspati ghee. Vanaspati ghee contains sesame oil, which is not present in desi ghee.
               The vendor adulterates the desi ghee with vanaspati to gain profit. Sesame oil reacts with mixture of conc. HCl and furfural solution to produce rose red colour.this test is known as Baudouin test.
FIG.2             
EXPERIMENT NO. 2
REQUIREMENTS:(i)A Test tube (ii)Conc. HCl (iii)2% furfural in alcohol (iv)Sample
PROCEDURE:
Take about 5 ml of melted ghee sample in a test tube . Add 5 ml conc. HCl followed by the addition of 2-3 drops of 2% solution of furfural in alcohol. Shake the mixture and allow
 to stand for about 10 minutes. Appearance of rose red color indicates the presence of vanaspati ghee in the ghee sample.
      
ANNAPURNA GHEE,BATCH NO. 1101/0921/C1
OPEN SAAMPLE
ADULTERANTS NOT FOUND
ADULTERANTS NOT  FOUND
                                                        
  2.3 DETECTION OF STARCH IN MILK
             Milk is the most approved food. It is so pure that a newborn child gets a taste of it as its first food. It is highly nutritious and extremely good for the body. But a food like this has also made impure by vendors adulterating   it with adulterants such as starch. The vendor acquires profit from it harming its nutritional values.
                        Milk  consists  of  three  basic  components  which are water (80%) , fat (3.5%)  ,and solids containing protein , lactose  and  mineral matters (8.5%). Milk is adulterated   with starch   to maintain  the  thickness of   fat   extracted milk or diluted milk. Starch can be detected by adding iodine solution to milk
.
EXPERIMENT NO. 3 
REQUIREMENTS: (i) A Test tube (ii) Iodine solution (iii) Sample.
PROCEDURE:    
             Take 5ml of milk sample in a test tube and boil it for 3-4 minutes. Cool the sample and add 1 or 2drops of iodine   solution and shake the content. Appearance of blue color indicates presence of starch in the sample.





COW MILK
AMUL TAAZA,BATCH NO.1101/9102/V3,MANUFACTURED DATE:NOV/11
ADULTERANTS NOT FOUND
ADULTERANTS NOT FOUND

  2.4 DETECTION OF METANIL YELLOW IN TURMERIC
POWDER
              Turmeric powder(Haldhi) is a popular dye used in cooked food. It is often adulterated  with a cheap dye called metanil yellow which is responsible for the cause of cancer, to increase its quantity and gain profit. A few drops of conc. HCl is used to detect metanil yellow.
EXPERIMENT NO.4
REQUIREMENTS: (i)A Test tube (ii)Conc. HCl (iii) Sample.
PROCEDURE:
1.Detection of chalk powder
                  A small amount of given sample was taken in a test tube & about ml of dil. HCl was added to it. No effervescence indicates the absence of chalk powder.


2.Detection of brick powder

                 A small amount of given sample was taken in a test tube & about ml of CCl4 was added to it.


3.Detection of metanil yellow

                
         
          Take a small amount of turmeric powder in a watch glass and add 2-4 drops of dil. HCl to it. If pink colour appears and spreads on addition of few drops indicates the presence of metanil yellow.





OPEN SAMPLE
HONEE TURMERIC POWDER,BATCH NO.1108/2450/B5,MANUFACTURED DATE:JUN/11

ADULTERANT FOUND
ADULTERANT NOT FOUND



     2.5 DETECTION OF ADULTERANTS IN CHILLY POWDER
         Chilly powder is a popular dye used in cooked food. It is often adulterated with red lead salts or brick powder.It can be detected by adding few drops of nitric acid to the sample.

EXPERIMENT NO: 5                                                       
REQUIREMENTS:- A glass, water, dil. Nitric acid.
PROCEDURE:-
1.Adulteration of red lead salts
                    To a sample of chilly powder, dil. Nitric Acid was added. The solution was filtered and two drops of potassium iodide  were added into it. No yellow ppt. indicated the absence of lead salts in a chilly powder.


2.Adulteration of brick powder

                   A small amount of given red chilly powder was added in a beaker containing water. Settling of some powder at the bottom & floating pure chilly powder over water indicates the presence of brick powder in a given sample


RAJAH CHILLY POWDER ,BATCH NO.5610/6722/B7,MANUFACTUERED DATE:NOV/11
OPEN SAMPLE
ADULTERANT NOT FOUND
ADULTERANTS FOUND






  2.6 DETECTION OF DUST PARTICLES IN ATTA 
S
EXPERIMENT NO:6
REQUIREMENTS:- Test tube, CCl4.
PROCEDURE:-
    Take a sample of atta in a test tube. Add some amount of Ccl4 in the test tube.If ppt is seen then dust particles are present in the atta.

ASHIRBAD ATTA,BATCH NO.1102/0928/V1,MANUFACTURED DATE:AUG/11
OPEN SAMPLE
ADULTERANTS NOT FOUND
ADULTERANTS  FOUND
                                                                                                                                
ADDITIONAL  ADULTERANT(CHEMICAL).

                 MSG or Monosodium glutamate is a common adulterant used in chicken( specially in restaurants) for flavor. But it is actually quite harmful. It directly effects the brain. It causes destruction of brain cells which also leads to slow loss of memory.
           It also causes artificial hunger in human beings and makes us want to eat more. As such the normal production of enzymes is interrupted which is harmful for appetite and also normal growth in the body.





                                                                                                                                                                                                                                                                                             
                                              

              CONCLUSION
      Selection of wholesome and non-adulterated food is essential for daily life to make sure that such foods do not cause any health hazard. Visual examination of the food before purchase makes sure to ensure absence of insects, visual fungus, foreign matters, etc. Therefore, due care taken by the consumer at the time of purchase of food after thoroughly examining can be of great help. Secondly, label declaration on packed food is very important for knowing the ingredients and nutritional value. It alsohelps in checking the freshness of the food and the period of best before use. The consumer should avoid taking food from an unhygienic place and food being prepared under unhygienic conditions. Such types of food may cause various diseases. Consumption of cut fruits being sold in unhygienic conditions should be avoided. It is always better to buy certified food from reputed shop…………………………………

                                                        
              
REFERENCE
.“Manual Of Modern Chemistry” --------- DR. A K Baruah
                                                                DR. P M Saikia
                                                      Publishing Year-2010
                                                               Page  no. 80-81                                 
                                                ISBN NO. 81-86384-87-1

“Senior Secondary Practical Chemistry”- DR. K Choudhury
                                                         DR. S K Choudhury
                                                     Publishing Year- 2011
                                                             Page no.175-176
    .WIKIPEDIA.
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